Development of titanium-based certified reference materials

نویسندگان

چکیده

The Institute for Certified Reference Materials (ICRM) issued the first time certified reference materials (CRM 11777-2021) of mass fraction hydrogen, oxygen and nitrogen in titanium-based materials, i.e., titanium alloy 2V (ISO 1-1) VT 1-00 1-2). finished material is presented form cylinders 2.5 mm diameter 5-6 height. a cylinder about 0.1 g. To certify gas-forming elements, we used methods fusion under inert gas flow (hydrogen, oxygen, nitrogen) high-temperature vacuum extraction with spectroscopy (hydrogen). analyzers were calibrated using CRM, dose (for hydrogen), substance constant stoichiometric composition (potassium nitrate). Conditions determination alloys an ELTRA ONH-2000 analyzer solid have been refined analytical laboratory ICRM. accuracy indicators (assigned characteristics) measurement procedure determined great bulk experimental data.

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ژورنال

عنوان ژورنال: ????????? ???????????. ??????????? ??????????

سال: 2023

ISSN: ['1028-6861', '2588-0187']

DOI: https://doi.org/10.26896/1028-6861-2023-89-2-ii-70-76